Hints for Analysing Volatile Organics

RESTEK Technical Notes Hints for Analysing Volatile Organics p1-27 complete PDF
approx 920k page-served



Contents include . . .
  • An Overview of EPA Methodology for VOAs and Purge & Trap.
  • Techniques for Interfacing Capillary Columns to Purge & Trap and Detection Systems.
  • Capillary Columns Recommendations
    for VOA.
  • Suggestions for Optimising Capillary Column Operating Conditions.
  • Common Problems Associated with VOAs
     

Methods Overview . . . 2
Drinking Water
Waste Water
Hazardous Water . . . 3

Purge & Trap Overview . . .4

  • P&T Components  . . .4
  • Adsorbent Material and Traps . . . 5
  • Water Management Systems
  • Sequences and Flow Paths of the P&T Unit . . 6
  • and More. . . 7 . . . 8

GC Configurations

  • Wide Bore Systems and More . . . 9
  • Narrow Bore Systems . . . 10
    Cryofocusing . . . 10
  • Injection Port Splitting . . . 11
  • P&T Interfacing to the System . . . 12
  • Injection Port Connection . . . 12
  • Direct Connection; Low Volume Injectors . . . 13

Capillary Columns   Rttx-502.2 . . . 14

  • Rtx-624, Rtx-1  . . . 15
  • Retention Times . . . 16
  • Detection Systems . . . 17
    PID/ELCD(Hall) Detectors . . . 17
    GC/MS Operation . . . 18 and More . . .19

System Calibration / Troubleshooting . . . 19

  • Common Problems Associated with P&T Units . . . 20
  • Common Problems Associated with the GC System . . . 21 and More . . . 22

Product Listing

  • Columns, Transfer Lines, Sparging Vessels . . . 23
  • Low Volume Injectors . . . 24
  • ELCD Supplies; Syringes . . . 25
  • Restek's Leak Detective . . . 26
  • VOA-CYL and Chemical Standards . . . 27

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